| 書目名稱 | Organotrifluoroborate Preparation, Coupling and Hydrolysis | | 編輯 | Alastair J. J. Lennox | | 視頻video | http://file.papertrans.cn/705/704546/704546.mp4 | | 概述 | Nominated as an outstanding Ph.D. thesis by the University of Bristol, UK.Includes an extensive review on organotrifluoroborate salts.Demonstrates a new, simple and etch-free preparation method for or | | 叢書名稱 | Springer Theses | | 圖書封面 |  | | 描述 | Alistair Lennox‘s thesis reports on the reactivity of organotrifluoroborates, which are becoming increasingly important reagents in synthesis. The thesis is divided into three sections. The first section describes a method for preparing organotrifluoroborates. The second section reports on a mechanistic investigation into the main application of RBF3K reagents as coupling partners in Suzuki-Miyaura coupling, phenomena identified as arising from organotrifluoroborate hydrolysis and fluoride release. The final section reports on a detailed investigation into the hydrolysis mechanism, a prerequisite for their Suzuki-Miyaura coupling, and how it may be predicted and controlled. This research has uncovered many interesting and useful details and shows how problems associated with Suzuki-Miyaura coupling can best be addressed. There has already been wide industrial uptake of the new procedures and insights. The broad nature and clear and succinct style will make the thesis a valuable resource for anyone working in synthesis, organometallic chemistry, or in homogeneous catalysis. | | 出版日期 | Book 2013 | | 關(guān)鍵詞 | Cross-coupling; Glassware Etching; Kinetics of Hydrolysis; Organotrifluoroborate Salts; Side-product Sup | | 版次 | 1 | | doi | https://doi.org/10.1007/978-3-319-01134-9 | | isbn_softcover | 978-3-319-37734-6 | | isbn_ebook | 978-3-319-01134-9Series ISSN 2190-5053 Series E-ISSN 2190-5061 | | issn_series | 2190-5053 | | copyright | Springer International Publishing Switzerland 2013 |
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